Efficient and one-pot synthesis of novel sulfamates from carboxylic acids

Atmaca, Ufuk

doi:10.1016/j.tet.2019.130467

Makale Tam Makale Uluslararası 2019 Açık erişimli

Efficient and one-pot synthesis of novel sulfamates from carboxylic acids

Ufuk Atmaca

TETRAHEDRON Cilt 75 · Sayı 34 · 23.08.2019

DOI ile aç

Özet

Effective synthesis of novel sulfamates from various carboxylic acids has been developed in the presence of chlorosulfonyl isocyanate (CSI) in mild conditions. Several acids, bases and solvents effects were investigated for one-pot synthesis sulfamates as a catalyst. Finally, triflic acid was found to possess efficiently under optimized conditions in acetonitrile. This method is easy, fair price and practical. It can be synthesized on grams and milligrams scale. (C) 2019 Elsevier Ltd. All rights reserved.

Anahtar kelimeler

INHIBITORS ANALOGS chlorosulfonyl isocyanate Sulfamate Carboxylic acid Triflic acid

Atıf için künye

Atmaca, U. (2019). Efficient and one-pot synthesis of novel sulfamates from carboxylic acids. TETRAHEDRON, 75(34). https://doi.org/10.1016/j.tet.2019.130467

BibTeX

@article{atmaca2019-72495,
  author = {Atmaca, Ufuk},
  title = {Efficient and one-pot synthesis of novel sulfamates from carboxylic acids},
  journal = {TETRAHEDRON},
  year = {2019},
  volume = {75},
  number = {34},
  issn = {0040-4020},
  doi = {10.1016/j.tet.2019.130467},
  url = {https://akademik.atauni.edu.tr/yayinlar/72495-efficient-and-one-pot-synthesis-of-novel-sulfamates-from-carboxylic-acids}
}