Synthesis and Characterization of a Novel Conformation of 2,9,10-Tribromoanthracene-1,4-dione
Özet
Synthesis and X-ray analysis of single crystals of 2,9,10-tribromoanthracene-1,4-dione 4 has been described and its novel conformation is reported. Single crystals were grown by slow evaporation technique from toluene solution at -15 A degrees C. The compounds have been characterized by elemental analysis, FT-IR, Mass and NMR spectroscopy. The compound crystallizes in the triclinic space group P-1 with unit cell dimensions a = 7.6842(2), b = 9.4865(2), c = 19.9388(4) , alpha = 78.784(5), beta = 76.980(5), gamma = 67.834(4) ; V: 1,301.75(7) (3); Z = 2, R (1) = 0.0748, and wR (2) = 0.131.
Atıf için künye
BERKİL AKAR, K., ÇAKMAK, O., & Şahin, E. (2013). Synthesis and Characterization of a Novel Conformation of 2,9,10-Tribromoanthracene-1,4-dione. JOURNAL OF CHEMICAL CRYSTALLOGRAPHY, 43(12), 677–684. https://doi.org/10.1007/s10870-013-0472-4
BibTeX
@article{berkilakar2013-66658,
author = {BERKİL AKAR, KIYMET and ÇAKMAK, Osman and Şahin, Ertan},
title = {Synthesis and Characterization of a Novel Conformation of 2,9,10-Tribromoanthracene-1,4-dione},
journal = {JOURNAL OF CHEMICAL CRYSTALLOGRAPHY},
year = {2013},
volume = {43},
number = {12},
pages = {677--684},
issn = {1074-1542},
doi = {10.1007/s10870-013-0472-4},
url = {https://akademik.atauni.edu.tr/yayinlar/66658-synthesis-and-characterization-of-a-novel-conformation-of-2910}
}