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Makale Tam Makale Uluslararası 2007

2-Hydroxy-N-(3-oxo-1-thia-4-azaspiro[4.5]dec-4-yl)-2,2-diphenylacetamide

Mehmet Akkurt, Selvi Karaca, Ertan Şahin, Oezlen Guezel, Aydin Salman, Eser Ilhan

ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE Cilt 63 · 01.08.2007
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Özet

In the molecule of the title compound, C(22)H(24)N(2)O(3)S, the dihedral angle between the two phenyl rings is 70.28 (11)degrees. The cyclohexane ring adopts a chair conformation while the thiazolidine ring assumes an envelope conformation. The crystal packing is stabilized by intramolecular N-H center dot center dot center dot O and intermolecular C-H center dot center dot center dot O and O-H center dot center dot center dot O hydrogen-bonding interactions. The structure also contains C-H center dot center dot center dot Cg interactions, where Cg is the centroid of the phenyl ring at (1-x, -y, 1-z); for this contact, C center dot center dot center dot Cg = 3.721 (3) angstrom, H center dot center dot center dot Cg = 2.82 angstrom and C-H center dot center dot center dot Cg = 162 degrees.

Atıf için künye

Akkurt, M., Karaca, S., Şahin, E., Guezel, O., Salman, A., & Ilhan, E. (2007). 2-Hydroxy-N-(3-oxo-1-thia-4-azaspiro[4.5]dec-4-yl)-2,2-diphenylacetamide. ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 63. https://doi.org/10.1107/s1600536807031650

BibTeX
@article{akkurt2007-66654,
  author = {Akkurt, Mehmet and Karaca, Selvi and Şahin, Ertan and Guezel, Oezlen and Salman, Aydin and Ilhan, Eser},
  title = {2-Hydroxy-N-(3-oxo-1-thia-4-azaspiro[4.5]dec-4-yl)-2,2-diphenylacetamide},
  journal = {ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE},
  year = {2007},
  volume = {63},
  issn = {1600-5368},
  doi = {10.1107/s1600536807031650},
  url = {https://akademik.atauni.edu.tr/yayinlar/66654-2-hydroxy-n-3-oxo-1-thia-4-azaspiro45dec-4-yl-22-diphenylacetamide}
}