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Makale Tam Makale Uluslararası 2017

Synthesis and characterization of new thiadiazole derivatives bearing a pyrazole moiety

Mustafa Sacmaci, Ciler Arslaner, Ertan Şahin

PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS Cilt 192 · Sayı 10 · ss. 1134–1139 · 01.01.2017
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Özet

A series of thidiazole derivatives (4, 7) from pyrazole-3-carboxylic acid chloride (2) and pyrazole-3,4-dicarboxylicacid chloride derivatives (6) were synthesized and characterized. The structures of the new compounds were confirmed byelemental analysis, NMR (H-1 and C-13) and IR spectra. The molecular and crystal structure of 4-benzoyl-N-[5-(methylthio)-1,3,4-thiadiazol-2-yl]-1,5-di-phenyl-1H-pyrazole-3carboxamide(4d)was determined by single crystal X-ray diffraction method.

Anahtar kelimeler

ACID Pyrazole Thiadiazole X-ray structure

Atıf için künye

Sacmaci, M., Arslaner, C., & Şahin, E. (2017). Synthesis and characterization of new thiadiazole derivatives bearing a pyrazole moiety. PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS, 192(10), 1134–1139. https://doi.org/10.1080/10426507.2017.1345905

BibTeX
@article{sacmaci2017-66596,
  author = {Sacmaci, Mustafa and Arslaner, Ciler and Şahin, Ertan},
  title = {Synthesis and characterization of new thiadiazole derivatives bearing a pyrazole moiety},
  journal = {PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS},
  year = {2017},
  volume = {192},
  number = {10},
  pages = {1134--1139},
  issn = {1042-6507},
  doi = {10.1080/10426507.2017.1345905},
  url = {https://akademik.atauni.edu.tr/yayinlar/66596-synthesis-and-characterization-of-new-thiadiazole-derivatives-bearing-a-pyrazole}
}