A Facile and Catalyst-free Synthesis of Hexahydroacridine-1,8(2H,5H)-dione and Octahydroacridin-10(1H)-yl)thiourea Derivatives: Inter- and Intramolecular Aza-Michael addition
Özet
An easy and convenient technique for the one-pot synthesis of novel compounds of hexahydroacridine-1,8(2H,5H)-dione and octahydroacridin-10(1H)-yl) thiourea derivatives has been developed by the reaction of the octahydro-1H-xanthenes with hydroxylamine hydrochloride and thiosemicarbazide in ethylene glycol, which is a green solvent, under mild reaction conditions. IR, H-1 NMR, C-13 NMR spectrometry, and X-ray diffraction analysis were used to identify the structures of these compounds.
Atıf için künye
Pesyan, N. N., Akhteh, N., Batmani, H., Anıl, B., & Şahin, E. (2020). A Facile and Catalyst-free Synthesis of Hexahydroacridine-1,8(2H,5H)-dione and Octahydroacridin-10(1H)-yl)thiourea Derivatives: Inter- and Intramolecular Aza-Michael addition. HETEROCYCLIC COMMUNICATIONS, 26(1), 26–32. https://doi.org/10.1515/hc-2020-0005
BibTeX
@article{pesyan2020-66576,
author = {Pesyan, Nader Noroozi and Akhteh, Narmin and Batmani, Hana and Anıl, Barış and Şahin, Ertan},
title = {A Facile and Catalyst-free Synthesis of Hexahydroacridine-1,8(2H,5H)-dione and Octahydroacridin-10(1H)-yl)thiourea Derivatives: Inter- and Intramolecular Aza-Michael addition},
journal = {HETEROCYCLIC COMMUNICATIONS},
year = {2020},
volume = {26},
number = {1},
pages = {26--32},
issn = {0793-0283},
doi = {10.1515/hc-2020-0005},
url = {https://akademik.atauni.edu.tr/yayinlar/66576-a-facile-and-catalyst-free-synthesis-of-hexahydroacridine-182h5h-dione-and}
}