Preparation of PbS and PbO nanopowders from new Pb(II)(saccharine) coordination polymers
Özet
Nanopowders and single crystal of new Pb(II) three-dimensional coordination polymer, [Pb(H2O)(mu-OAc)(mu-sac)(n), "PASAC" were synthesized by a sonochemical and branched tube methods (Yilmaz et al., Z. Anorg. Allg. Chem. 629 (2003) 172). The new nano-structures of Pb(II) coordination polymer were characterized by X-ray crystallography analysis, scanning electron microscopy (SEM), X-ray powder diffraction (XRD), surface analysis (BET), and IR spectroscopy. The crystal structure of these compounds consists of three-dimensional polymeric units. The thermal stability of compounds was studied by thermal gravimetric analysis (TGA) and differential thermal analyses (DTA). PbS and PbO nano-structures were obtained by calcinations of the nano-structures of this coordination polymer at 600 degrees C. (C) 2014 Elsevier B.V. All rights reserved.
Atıf için künye
Aslani, A., Musevi, S. J., Şahin, E., & YILMAZ, V. T. (2014). Preparation of PbS and PbO nanopowders from new Pb(II)(saccharine) coordination polymers. APPLIED SURFACE SCIENCE, 318, 206–212. https://doi.org/10.1016/j.apsusc.2014.03.088
BibTeX
@article{aslani2014-66528,
author = {Aslani, Alireza and Musevi, Seyid Javad and Şahin, Ertan and YILMAZ, VEYSEL TURAN},
title = {Preparation of PbS and PbO nanopowders from new Pb(II)(saccharine) coordination polymers},
journal = {APPLIED SURFACE SCIENCE},
year = {2014},
volume = {318},
pages = {206--212},
issn = {0169-4332},
doi = {10.1016/j.apsusc.2014.03.088},
url = {https://akademik.atauni.edu.tr/yayinlar/66528-preparation-of-pbs-and-pbo-nanopowders-from-new-pbiisaccharine-coordination}
}