Rapid Mass Spectrometric Study of a Supercritical CO2-extract from Woody Liana Schisandra chinensis by HPLC-SPD-ESI-MS/MS
Özet
Woody liana Schisandra chinensis contains valuable lignans, which are phenylpropanoids with valuable biological activity. Among green and selective extraction methods, supercritical carbon dioxide (SC-CO2) was shown to be the method of choice for the recovery of these naturally occurring compounds. Carbon dioxide (CO2) was the solvent with the flow rate (10-25 g/min) with 2% ethanol as co-solvent. In this piece of work operative parameters and working conditions were optimized by experimenting with different pressures (200-400 bars) and temperatures (40-60 degrees C). The extraction time varied from 60 to 120 min. HPLC-SPD-ESI -MS/MS techniques were applied to detect target analytes. Twenty-six different lignans were identified in the S. chinensis SC-CO2 extracts.
Anahtar kelimeler
Atıf için künye
Razgonova, M., Zakharenko, A., Pikula, K., Kim, E., Chernyshev, V., Ercişli, S., Cravotto, G., & Golokhvast, K. (2020). Rapid Mass Spectrometric Study of a Supercritical CO2-extract from Woody Liana Schisandra chinensis by HPLC-SPD-ESI-MS/MS. MOLECULES, 25(11). https://doi.org/10.3390/molecules25112689
BibTeX
@article{razgonova2020-264783,
author = {Razgonova, Mayya and Zakharenko, Alexander and Pikula, Konstantin and Kim, Ekaterina and Chernyshev, Valery and Ercişli, Sezai and Cravotto, Giancarlo and Golokhvast, Kirill},
title = {Rapid Mass Spectrometric Study of a Supercritical CO2-extract from Woody Liana Schisandra chinensis by HPLC-SPD-ESI-MS/MS},
journal = {MOLECULES},
year = {2020},
volume = {25},
number = {11},
issn = {1420-3049},
doi = {10.3390/molecules25112689},
url = {https://akademik.atauni.edu.tr/yayinlar/264783-rapid-mass-spectrometric-study-of-a-supercritical-co2-extract-from-woody-liana}
}