Atatürk Üniversitesi Atatürk Üniversitesi
Ara
Yayınlara dön
Makale Tam Makale Uluslararası 2010

Development of a multiresidue method for the determination of multiclass pesticides in soil using GC

Jong-Hyouk Park, Md. Iqbal Rouf Mamun, Jeong-Heui Choi, Abdelaty Mostafa Abdelaty Hassıbelnaby, M. E. Assayed, Woo Jung Choi, Kwang Sik Yoon, Seong-Soo Han, Hee Kweon Kim, Byung Jun Park, Kap Soon Kim, Sang Don Kim, Hun Geun Choi, Jae-Han Shim

Biomedical Chromatography Cilt 24 · Sayı 8 · ss. 893–901 · 01.01.2010
DOI ile aç

Özet

The principal objective of the present study was to develop a multiresidue analytical method for 62 pesticides in a soil matrix. Soil samples were fortified with known quantities of pesticides at two different concentration levels (0.1 and 0.01 mu g/g) and the analytes were extracted via a liquid-solid extraction method. The pesticides were separated on an HP5 capillary column and were detected by gas chromatography coupled to an electron capture detector (GC-ECD). The method was validated, considering its good linearities (r(2) = 0.978-0.999), specificity and recovery characteristics. Recoveries were found between 70.3 and 113.4% for all pesticides except edifenphos (67.5%) and dichlobenil (69.5%) spiked at a 0.1 mu g/mL concentration level and 74.5-117% except ethalfluralin (63.3%) and dichlobenil (51.9%) spiked at a concentration of 0.01 mu g/mL. The developed method could be utilized as a simple and cost-effective method for the routine analysis of 62 pesticides in soil samples. Copyright (C) 2009 John Wiley & Sons, Ltd.

Atıf için künye

Park, J., Mamun, M. I. R., Choi, J., Hassıbelnaby, A. M. A., Assayed, M. E., Choi, W. J., Yoon, K. S., Han, S., Kim, H. K., Park, B. J., Kim, K. S., Kim, S. D., Choi, H. G., & Shim, J. (2010). Development of a multiresidue method for the determination of multiclass pesticides in soil using GC. Biomedical Chromatography, 24(8), 893–901. https://doi.org/10.1002/bmc.1383

BibTeX 
@article{park2010-209507,
  author = {Park, Jong-Hyouk and Mamun, Md. Iqbal Rouf and Choi, Jeong-Heui and Hassıbelnaby, Abdelaty Mostafa Abdelaty and Assayed, M. E. and Choi, Woo Jung and Yoon, Kwang Sik and Han, Seong-Soo and Kim, Hee Kweon and Park, Byung Jun and Kim, Kap Soon and Kim, Sang Don and Choi, Hun Geun and Shim, Jae-Han},
  title = {Development of a multiresidue method for the determination of multiclass pesticides in soil using GC},
  journal = {Biomedical Chromatography},
  year = {2010},
  volume = {24},
  number = {8},
  pages = {893--901},
  issn = {0269-3879},
  doi = {10.1002/bmc.1383},
  url = {https://akademik.atauni.edu.tr/yayinlar/209507-development-of-a-multiresidue-method-for-the-determination-of-multiclass}
}